Throughout industry components are mixed in stirred vessels or pipes. The challenge is to determine exactly how well the ingredients are being mixed.

Conductivity maps for gas-liquid dispersion from a central sparger located at the bottom of the mixer for Rushton turbine (at 100 rpm) showing the effect of sparge rate (Williams et al., 1998).

Factors such as the composition and nature of the ingredients, the position, speed and design of the stirrer and the structure of the vessel all contribute to mixing effectiveness.

Any reduction in mixing effectiveness:

- may increase the mixing time with consequential reduction in capacity

- increase the energy consumption

- reduce the yield and quality of the downstream processes.

The challenge is to improve understanding and detailed knowledge of the mixing and hence improve performance and availability. Often the structure is complex and the nature of the ingredients and the operating conditions make visual inspection either impossible or hazardous.

In liquid-liquid mixing stirred tank 8 x 16-electrodes are used connected to an Industrial Tomography Systems p2+ instrument designed
and established to measure and display ERT data. Each 16-electrode ring of electrodes generates a conductivity map of the cross-section at that point as shown below:

In these circumstances gas is injected into the base of the mixer. For calibration a high conductivity tracer gas is injected in the base. The above illustration shows an example of three-dimensional images for gas injection into a liquid.

The colour red indicates a region of high gas hold-up with green/ yellow as intermediate hold-up.

Gas-liquid homogeneity-heterogeneity

7 liters/min - homogeneous

14 liters/min - heterogeneous

Key benefits include:

It has been widely demonstrated that ERT technology can be applied to a range of mixing processes. The benefits to the customers are:

  • At the R&D stage of mixing development, improved process understanding and validation of CFD models to aid process design and scale-up.
  • Through measurement improved control and product quality in industrial reactors.
  • Higher yields through improved mixing with shorter mixing time and less energy consumption.

Register to access our "Mixing" case studies available from the Download section on the right.

Register to access our "Mixing" case studies available from the Download section on the right.

Publications:

Hui, L.K., Bennington, C.P.J. and Dumont, G.A. (2009) Cavern formation in pulp suspensions using sideentering axial-flow impellers, Chemical Engineering Science, Vol. 64, pp 509-519

Mann, R, Wang, M, Forrest, AE, Holden, PJ, Dickin, FJ, Dyakowski, T and Edwards, RB (1999) Gas-Liquid and Miscible Liquid Mixing in a Plant-Scale Vessel Monitored Using Electrical Resistance Tomography, Chem. Eng. Commun., Vol. 175, pp 39-48

M. Wang, A. Dorward, D. Vlaev and R. Mann (2000) Measurements of gas-liquid mixing in a stirred vessel using electrical resistance tomography, Chemical Engineering Journal, Vol. 77, pp 93-98

For more information about this paper, please contact ITS.

In the Press:

  •  The Chemical Engineer Feb 2009 - Seeing is believing

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